Piston-cylinder apparatus with a working volume of 22 cm3 and pressure up to 23 kbar for ultra-high-pressure synthesis in the liquid phase.
In this paper, we provide a detailed description of a liquid-phase high-pressure apparatus with a working volume of 22 cm3 and a maximum pressure capacity of 23 kbar and temperatures up to 150 °C. Alongside the design of the ultra-high-pressure reactor, we also outline the structure of the three-layer steel reaction ch...